e-book Process Analytical Chemistry: Control, Optimization, Quality, Economy

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Just as accurate and reliable process variable measurements are critical for good process control, accurate chemical composition and other product quality measurements are critical for companies across a wide variety of process industries. While the required frequency of measurements will vary based on the process time dynamics, faster is often better. Off-line lab measurements can take hours or even days to complete, and at-line measurements can consume precious minutes; but in-line and on-line analyzers typically provide analysis measurements in real time or near-real time.

This enables operators and control systems to respond quickly to measurements that are varying from established parameters to minimize product rework, waste and quality giveaway; and increase flexibility by reducing the time it takes to start up processes, make product grade transitions or switch product recipes. As with most sophisticated technologies, technical and financial limitations apply when implementing real-time process analysis.

While the number of technologies and corresponding analytical measurements that have moved from the laboratory to the plant floor and into the process is growing; not all compounds and mixtures can be analyzed in real time or near real-time. And even when the technology is available, installing these systems comes at a price.

Integrating the analyzers and analysis results into real-time optimization schemes could help take users to the next level, but also involve additional integration, model building and support costs. Her expertise includes field devices, instrumentation, and process automation with a special interest in communication and new technologies. Constanze comes from a family of engineers and is an alumna of the University of Trier in Germany.

She has been working in technical publishing for over 15 years.

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Chemical Processing. Menu Newsletters Subscribe. Newsletters Subscribe. Follow us on:. Analytical Measurement Approaches Ideally, chemical composition or other product quality parameters should be made with a frequency and an accuracy high enough to enable automated feedback control.

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Off-Line Lab Analysis Historically, property and composition measurements for feedstocks, work in process or finished products were executed on product samples in dedicated laboratories after being collected manually from the process and brought back to the laboratory for conditioning and analysis. At-Line Analysis Automated analytical devices allow some measurements to be moved closer to the process. Produktbeschreibung Process Analytical Chemistry, like the whole field of analytical chemistry, plays an integral and essential role in every industrial company based on chemical processes.

It aids to decision making in the series of process steps, so its results have decisive technical, economic and ecological effects. This book is aimed at analytical practitioners, chemical engineers and process engineers who require information about the possibilities and the methods of process analytics and knowledge about their effectiveness and efficiency, e. In particular, the chemical engineers and chemical engineering technicians working in small and medium-sized companies are also included since they have to solve process analytical problems without an experienced analyst at their sides.

Therefore references to the literature and lists of suppliers are added to particular chapters, naturally these cannot make any claims to completeness, but they are intended as being helpful as an indication and enables practical problems to be solved more easily. In special chapters, examples of the interaction and the mutual dependence and the reciprocal influence of various disciplines are described.

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PROCESS ANALYTICAL CHEMISTRY. - Control, Optimization, Quality, Economy

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